Table 9

Formulation of emulsions prior to freeze-drying.

# Experiment Formulation Concentration Droplet Size after rehydration and 5’ stirring at 13000 rpm
1 Addition of glycerol 1% D[1.0] ≈ 2xD[1.0] native
2 Addition of mannitol 1% D[1.0] ≈ 4xD[1.0] native
3 Addition of Tris 0,075 M D[1.0] ≈ D[1.0] native
4 NaCl 3% washing of the emulsion No powder obtained but free oil exuding

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